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Material Drying 13 Aufrufe

Polyamic acid(PAA)solution viscosity control

Problembeschreibung
PAA solution viscosity is too high or too low to be processed normally by casting or coating
Ursachenanalyse
Improper control of polycondensation reaction degree (monomer ratio, reaction temperature and time); solvent water content affects the degree of polymerization
Lösung
Strictly control the equimolar ratio of dianhydride and diamine; control the reaction temperature at -5~10°C (low-temperature solution polycondensation); use dry solvent
Wichtigste Erkenntnis
The molecular weight and viscosity of PAA are the primary control parameters for PI processing
PAAsolution viscositypolycondensationmonomer ratiodry solvent

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